Synthesis And Characterization Of Silver Or Silver Sulfide Filled Poly(3-Hydroxybutyrate) Nanocomposites

Yeo , Siew Yean (2012) Synthesis And Characterization Of Silver Or Silver Sulfide Filled Poly(3-Hydroxybutyrate) Nanocomposites. Masters thesis, Universiti Sains Malaysia.

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Abstract

Ag and Ag2S hydrosols were synthesized via chemical reduction and reflux methods respectively. A simple aqueous to organic phase transfer technique was employed to transfer the Ag and Ag2S nanoparticles from the respective hydrosol into poly(3-hydroxybutyrate) [PHB] chloroform solution. The Ag and Ag2S nanoparticles were stabilized by the PHB polymer in the organosols. The presence of metallic Ag or the Ag2S particles in the newly formed nano-biocomposites were confirmed by the X-ray Diffraction (XRD) technique. The particles size of Ag and Ag2S were within 7-12 nm and 14-24 nm respectively. At low concentration of PHB, the shape of Ag particles was sphere while for Ag2S particles were hexagonal-like.

Item Type: Thesis (Masters)
Subjects: Q Science > QD Chemistry > QD1-999 Chemistry
Divisions: Pusat Pengajian Sains Kimia (School of Chemistry) > Thesis
Depositing User: ASM Ab Shukor Mustapa
Date Deposited: 12 Nov 2018 02:46
Last Modified: 12 Apr 2019 05:26
URI: http://eprints.usm.my/id/eprint/42856

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