Abbas, Salih Hamza
(2015)
Preparation And Immobilization Of
Palladium(ii) And Nickel(ii) Salen Complexes
Onto Mcm-41 From Rice Husk For
Suzuki-Miyaura And Oxidation Reactions.
PhD thesis, Universiti Sains Malaysia.
Abstract
MCM-41 daripada abu sekam padi (RHA) telah berjaya disintesis dangan
menggunakan cetiltrimetilammonium bromida sebagai agen pegasal melalui kaedah
sol-gel pada sahu 100 oC. MCM-41 telah difungsikan dengan 3-
kloropropiltrietoksisilana (CPTES) sebagai agen pencantuman dan pepejal yang
diperoleh dilabel sebagai Cl-MCM-41.
MCM-41 was successfully prepared from rice husk ash (RHA) using
cetyltrimethylammonium bromide as a directing agent via sol-gel method at 100 oC.
MCM-41 was functionalized with 3-chloropropyltriethoxysilane (CPTES) as a
functioning agent and the solid obtained was labeled as Cl-MCM-41.
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